A choice collection of rare secrets and experiments in philosophy as also rare and unheard-of medicines, menstruums and alkahests : with the true secret of volatilizing the fixt salt of tartar / collected and experimented by the honourable and truly learned Sir Kenelm Digby, Kt., Chancellour to Her Majesty the Queen-Mother ; hitherto kept secret since his decease, but now published for the good and benefit of the publick by George Hartman.
About this Item
Title
A choice collection of rare secrets and experiments in philosophy as also rare and unheard-of medicines, menstruums and alkahests : with the true secret of volatilizing the fixt salt of tartar / collected and experimented by the honourable and truly learned Sir Kenelm Digby, Kt., Chancellour to Her Majesty the Queen-Mother ; hitherto kept secret since his decease, but now published for the good and benefit of the publick by George Hartman.
Author
Digby, Kenelm, Sir, 1603-1665.
Publication
London :: Printed for the author, and are to be sold by William Cooper ..., and Henry Faithorns and John Kersey ...,
1682.
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Subject terms
Medicine, Magic, mystic, and spagiric.
Alchemy.
Link to this Item
http://name.umdl.umich.edu/A35968.0001.001
Cite this Item
"A choice collection of rare secrets and experiments in philosophy as also rare and unheard-of medicines, menstruums and alkahests : with the true secret of volatilizing the fixt salt of tartar / collected and experimented by the honourable and truly learned Sir Kenelm Digby, Kt., Chancellour to Her Majesty the Queen-Mother ; hitherto kept secret since his decease, but now published for the good and benefit of the publick by George Hartman." In the digital collection Early English Books Online. https://name.umdl.umich.edu/A35968.0001.001. University of Michigan Library Digital Collections. Accessed June 13, 2024.
Pages
A Real and True way to Volatilize the
Salt of Tartar, and Corporifie Spirit of
Wine, as it was wrought by a Noble Per∣son
beyond Sea, and by him Communicated
unto me.
HE took but lbj. of Tartar well Calci∣ned,
and dissolved it in the Air, free
from the Sun, then filtred, and congealed
in a Glass Vessel, then he Calcined it as the
Dutch-man doth (in the next Process) to
keep it glowing hot for six or eight hours,
then dissolved it again in the Air, and filtred,
descriptionPage 148
congealed, and calcined as before. He re∣peated
this ten times, then dissolved it in di∣stilled
Vinegar (he used Spanish and French
Vinegar;) the whole Secret (as he saith)
consisteth in well distilling of the Vinegar,
which must be done in B. M. but it must be
so gentle, that you may receive the flegm
by it self; and as soon as you perceive that
the drops come Acid, change the Recipient,
putting on another, and then distill the Spi∣rit
with a stronger fire, so that you may tell
eight or nine between every drop: Conti∣nue
distilling until it become like a Syrup,
then change the Recipient again, and distill
with a stronger fire until it begin to smell of
the fire, and that it be almost dry. Recti∣fie
this last and strongest part by it self, and
put it to the weaker part, (keeping the
flegm by it self for another use) and recti∣fie
it together so often until there remain
not the least spot at the bottom of the Glass
after the distillations, which must be to dry∣ness
every time, and every time in a clean
Retort: This is not a strong Spirit of Vine∣gar,
nor needs it be, but this will do the Work.
Then take ℥vij. or viij. of your Salt of Tar∣tar,
and dissolve it in as much of the said
Spirit, or more, as will dissolve it; let it
stand, and it will settle some black feces;
then filter it, and congeal, and calcine it as
descriptionPage 149
before, but not with so strong a fire; it must
be scarce red-hot, and one hour will suffice;
grind it while it is hot, and dissolve it again
in new distilled Vinegar as before, let the
feces settle, then filter it, congeal and cal∣cine
again as before. Repeat this, till it leave
no feces behind, which will be in Seven or
Eight times, if you have wrought well; then
when it is very dry, take ℥j. of it to make a
tryal, put it into a clean Glass body, and
pour upon it so much high rectified Spirit
of Wine, as will not only moisten it, but
that it be very thin; let it stand thus twenty
four hours close stopped in a very gentle
heat, that it may be but Blood-warm; then
distill with a gentle fire. If the Spirit stays,
and the flegm come away, then proceed with
the whole parcel; but if not, you must con∣tinue
the dissolution in distilled Vinegar,
Filtration, Coagulation, and Calcination,
as before, until you find (by trying) that
the Spirit stayeth with the Salt, which it will
do in a few times: Then proceed with the
rest of the parcel in the same manner as you
did with the Ounce; continue the imbibition
and distillation with Spirit of Wine so often,
till the Spirit of Wine come away as strong
as it was put on. Then here lyeth the Se∣cret,
to Sublime it: Dissolve the said Salt of
Tartar impregnated in the flegm of your
descriptionPage 150
distilled Vinegar, or in a very weak Spirit
of Wine, using no more of the dissolvent
than will dissolve it; shake them well toge∣ther,
and it will instantly dissolve all the best
and finest part of the Salt of Tartar, and
leave the course part of it, for that will not
so easily dissolve, Pour off the dissolution,
and filter it, then put it into a Cucurbite,
and distill off the flegm off the Vinegar, or
the weak Spirit of Wine, and then will the
dry Spirit, or Aqua Sicca ascend like the
purest Isickles dry that ever you saw; and
this is the true Volatile Salt of Tartar, and
Spirit of Wine, in forma Salis, and is the
Vegetable Menstruum, which will dissolve
leaf ☉ into an Oylish Substance in a very
gentle heat.
The Tartar which remaineth in the bot∣tom
of this Sublimation you must put to
that which was left undissolved by the flegm
of Vinegar, or weak Spirit of Wine, and
Proceed to fix more Spirit of Wine upon
that, being first Calcined, but not so long,
nor with so strong a fir•• as formerly; and
then dissolve it once in the Ai•••• and it will
leave more feces at this time than at any time
before; then filter and congeal, and dissolve
it in distilled Vinegar•• as before. And now
you shall do more in three times than you
did all the times before, for the Tartar is
descriptionPage 151
altered in its Nature; then proceed with it
as before, imbibing with S. V. And thus
you may fix as much S. V. as you please,
and Sublime as many pure and clear Crystals
as you please.
Note, That when your Spirit of Wine is
fixed on the Tartar, it will be as sweet as
Sugar; but when it is separated, as above-said,
the Tartar will be of its old Nature,
but fit to be impregnated again with much
less trouble.
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